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The Need for Low Energy Profiling

The requirement for high depth resolution dynamic SIMS arises from the reduction in device size in the semiconductor industry. With the use of low implantation energies and new technology dependent on delta-doping and sharp interfaces, it is increasingly important to have access to depth profiling techniques which can quantify these structures both accurately and reproducibly.

When profiling with energetic oxygen beams, the kinetic energy of the incident particles is transferred to the near surface region of the sample, creating an altered layer in which atomic mixing has occurred. The depth of this layer is approximately 4nm per keV for an O2+ beam, and this imposes an absolute limit on depth resolution. Hence, it is necessary to use energies well below 1keV for profiling of shallow junctions.

Another important factor in the analysis of shallow implants is the transient region which occurs at the surface and at matrix interfaces. At the beginning of a shallow profile, the ion and sputter yields vary rapidly as probe atoms are incorporated into the analysed surface, and the surface chemistry changes. Similar effects occur at matrix interfaces. While this behaviour persists the depth profile is not quantifiable, and any features lying within the transient will be distorted. The thickness of the region, and hence the amount of lost information, can be reduced by using low impact energies.



The Principle of the Floating Ion Gun

In a conventional ion gun, ions are transported through almost the whole ion-optical column at an energy determined by the anode voltage. Thus, to attain a 250 eV impact energy (on a grounded sample) the anode must be set to 250 V and the beam travels through the column at this energy. At such low energy, space charge effects and aberrations of the wide beam seriously limit the final intensity of the probe and impair the probe shape.

In the floating ion gun, almost all of the column is floated to a negative potential and the beam is accelerated to a more viable transport energy between the extraction region and the final lens. Inside the final lens, the beam is decelerated to the desired impact energy. Thus, for a 250 eV impact energy, the anode is set to 250 V and the float could be -3 kV giving a transport energy of 3.25 keV. This provides a significant reduction in beam aberrations. In the FLIG, the Wien filter electrostatic plates and alignment units (including a bend to reject neutrals) are all referenced to the float voltage.



High Erosion Rate, Even at Low Energy

Shallow junction profiling requires the use of a low energy primary beam in order to minimise the effects of atomic mixing induced by the beam. As sputter yield reduces with lower energies, it is vital that the low energy probe has a high current density. Figure 1 shows characteristic plots of probe size versus beam current for the FLIG 5.

The FLIG 5’s high brightness duoplasmatron source and floating column optics deliver exceptional probe intensity, in comparison with conventional systems, facilitating low energy profiling with acceptable erosion rates.



High Depth Resolution and Dynamic Range

To attain high depth resolution without sacrificing erosion rate, the bottom of the analysis crater must remain flat through the profile. A good probe shape, with minimum aberration tails, is essential to minimise curvature at the sides of the crater. Reducing the extent of this curvature enhances depth resolution and dynamic range, as well as allowing the use of smaller scan fields and hence shorter analysis time.

Current vs spot size for the FLIG

Figure 1. Current vs spot size for the FLIG® 5.

The FLIG’s floating column transports the beam through most of the optics at high energy (generally between 2.5keV and 5keV). This greatly assists in reducing beam spreading in the column and concomitant aberrations in the probe. The result is sub-nanometre depth resolution at low energy, with profiles showing high dynamic range at all energies.

The depth resolution capability is demonstrated in Figure 2, which shows profiles of a Si-Ge superlattice. Grown by MBE, this structure has alternating 1nm layers of Si and Ge. The low energy profile shows a 45% valley between Ge peaks 14 and 15, showing the feature to be easily resolved.

Depth profiles of SiGe lattice

Figure 2. Depth profiles of SiGe lattice

A remarkable feature is the apparent increase in resolution with depth in the low energy profile. A cross-sectional TEM image of the sample revealed that the upper layers were buckled, causing the lower resolution of the top layers.



Ease of Operation

Control of the voltage settings in the FLIG is greatly simplified by the use of a computer software interface. This allows many useful features to be built into software, the most valuable being the facility to save complete sets of operating voltages. Critical control voltages such as extraction and alignment are referenced to other supplies rather than ground to simplify tuning of the column.

The system is ready for use with automated systems which can command a change of preset conditions, when required, using ASCII commands.

Beam Energy Range:200 eV to 5 keV
Max. Current (5 kV):> 500 nA
Min. Spot Size (5 kV, 500 nA):< 15 μm
Max. Current (1 kV):> 350 nA
Min. Spot Size (1 kV, 100 nA):< 25 μm
Max. Current (250 eV):> 250 nA
Min. Spot Size (250 eV, 100 nA):< 50 μm

IOG-30D Duoplasmatron Ion Beam System

IOG 30D

IOG 30D

30kV Duoplasmatron Ion Beam


The IOG 30D is a high-brightness focused ion beam system for contaminant free micro-machining or analysis of small areas. It uses a duoplasmatron ion source and two-lens optical column to produce a high-brightness, low-aberration spot. The source may run on pure argon (or other noble gases), nitrogen, or oxygen, and a mass filter is included in the column to separate beams of different mass/charge species. A selection of 5 apertures allows a wide current range. A gate valve in the column allows the source to be serviced without venting of the whole column.

Highlights

  • 30 kV High-Brightness Duoplasmatron Source
  • 500 nA Maximum Current
  • 500 nm Spot Size
  • Integrated Mass Filter
  • Runs on Ar, Ne, He, Kr, O2, & N2

Installation Requirements

The IOG 30D is designed for retrofitting to vacuum chambers of electron microscopes or SIMS instruments. It mounts via an NW63CF flange, either directly onto an instrument CF flange with clearance boltholes, or via a spacer to adapt to an O-ring flange. The column includes a 2° bend to reject any neutrals in the beam. So, the lower column projects into the instrument chamber off centre by ~6 mm, and angles towards the port axis such that it intersects the sample on the centreline.

The flange to end of column distance can be adapted at the time of manufacture, and can be set between 188 mm and 210 mm. The distance from the end of the column to the sample should ideally be between 18 and 25 mm.

The upper chamber of the ion column requires differential pumping, ideally via a 60 ls-1 turbo pump.

The gas supply must be a high purity (99.999%) with low water content for good performance. This is to be connected to a 6 mm stainless steel tube at the source. Noble gases can be switched off when not in use, Oxygen should be run continuously.



Electronics

The IOG 30D includes a 6U high voltage power supply for installation in a standard 19 inch rack. This provides the arc supply for the Duoplasmatron and all high voltage and static deflector supplies for the column.

Control is via a software interface, provided on cd for pc installation.

A suitable beam scanning system should be connected to the column. A system for secondary electron detection and imaging is also needed. Ionoptika offers these or we can advise on connections for alternative systems.

SED imaging with 30 keV helium beam, 50pA, achieving 100 nm spatial resolution

Figure 1. SED imaging with 30 keV helium beam, 50pA, achieving 100 nm spatial resolution. Image courtesy of National Institute for Materials Science, Japan.

Beam Energy Range:5 to 30 keV
Source Lifetime:> 400 hrs
Beam Stability:< ±2% / hour after 2 hour warm up
Max. Beam Current (Ar+ @ 30 KV):> 500 nA
Min. Spot Size (Ar+ @ 30 KV):< 500 nm
Mass filter:Yes
Column Isolation Valve:Yes