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IOG 30D

February 21, 2018/in News

IOG 30D

30kV Duoplasmatron Ion Beam

The IOG 30D is a high-brightness focused ion beam system for contaminant free micro-machining or analysis of small areas. It uses a duoplasmatron ion source and two-lens optical column to produce a high-brightness, low-aberration spot. The source may run on pure argon (or other noble gases), nitrogen, or oxygen, and a mass filter is included in the column to separate beams of different mass/charge species. A selection of 5 apertures allows a wide current range. A gate valve in the column allows the source to be serviced without venting of the whole column.

Highlights

30 kV High-Brightness Duoplasmatron Source
500 nA Maximum Current
500 nm Spot Size
Integrated Mass Filter
Runs on Ar, Ne, He, Kr, O₂, & N₂

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Details Key Features

Installation Requirements

The IOG 30D is designed for retrofitting to vacuum chambers of electron microscopes or SIMS instruments. It mounts via an NW63CF flange, either directly onto an instrument CF flange with clearance boltholes, or via a spacer to adapt to an O-ring flange. The column includes a 2° bend to reject any neutrals in the beam. So, the lower column projects into the instrument chamber off centre by ~6 mm, and angles towards the port axis such that it intersects the sample on the centreline.

The flange to end of column distance can be adapted at the time of manufacture, and can be set between 188 mm and 210 mm. The distance from the end of the column to the sample should ideally be between 18 and 25 mm.

The upper chamber of the ion column requires differential pumping, ideally via a 60 ls^-1 turbo pump.

The gas supply must be a high purity (99.999%) with low water content for good performance. This is to be connected to a 6 mm stainless steel tube at the source. Noble gases can be switched off when not in use, Oxygen should be run continuously.

Electronics

The IOG 30D includes a 6U high voltage power supply for installation in a standard 19 inch rack. This provides the arc supply for the Duoplasmatron and all high voltage and static deflector supplies for the column.

Control is via a software interface, provided on cd for pc installation.

A suitable beam scanning system should be connected to the column. A system for secondary electron detection and imaging is also needed. Ionoptika offers these or we can advise on connections for alternative systems.

Figure 1. SED imaging with 30 keV helium beam, 50pA, achieving 100 nm spatial resolution. Image courtesy of National Institute for Materials Science, Japan.

Beam Energy Range:	5 to 30 keV
Source Lifetime:	> 400 hrs
Beam Stability:	< ±2% / hour after 2 hour warm up
Max. Beam Current (Ar⁺ @ 30 KV):	> 500 nA
Min. Spot Size (Ar⁺ @ 30 KV):	< 500 nm
Mass filter:	Yes
Column Isolation Valve:	Yes

IOG 25GA

February 19, 2018/in News

IOG 25GA

Focused Liquid Metal Ion Beam

The IOG 25GA is a high performance 25 kV gallium ion beam system, designed for use in micro-machining and imaging SIMS applications. It offers a wide current range with a fine probe down to 50 nm, with either DC or pulsed operation. A PC control interface allows easy setup and monitoring of the system.

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Key Features

Gallium liquid metal ion source
Extremely small spot size of 50 nm.
High current option for 50 nA
High speed pulsing option
Pulse bunching option, for short intense pulses

Details Specifications

Overview

The IOG 25GA delivers a focused beam with beam energy of up to 25 keV. The wide current range enables the system to be used in a variety of applications from high precision direct write to large area quadrupole SIMS. In the lower current range, spatial resolution down to 50nm is achievable, subject to platform stability.

The assembly is configured for ease of installation as an instrument upgrade, with feedthroughs clustered together to allow minimum mechanical interference. A range of versions is available to accommodate different flange sizes or port lengths, and the column can be conventionally pumped or differentially pumped.

Ion Optics

The assembly consists of a gallium liquid metal ion source and a high precision two-lens optics assembly, illustrated in figure 1. There are manual and motorised options for aperture selection.

The IOG 25GA can be operated in collimated mode or in crossover mode, in which an intermediate field image is produced between the lenses. In this mode it can be set up for minimum motion blanking for TOF-SIMS.

The crossover mode can also be used in DC operation as a variable probe current mode, controlling the beam current by moving the intermediate image along the optical axis.

Electronics

The IOG 25GA power supply unit is a 6U rack-mountable 19 inch box. This provides all the high voltage and static deflector voltages required by the system. A sophisticated control software package is included; this can be installed on a PC running Windows 7 or higher.

Schematic of IOG25GA Ion Optics

Performance

The IOG 25 gives excellent spatial resolution throughout its current range, from micron performance at over 10 nA of beam current to below 50 nm in low current mode. It should be noted that the small spot performance requires a stable instrument platform with suitable isolation from vibration.

Figure 2 is a secondary electron image of a 12.5 micron copper grid, showing features below 50 nm across at a 25 mm working distance. A larger scan field can be achieved with a ± 200 V scan at greater working distances, as shown in Figure 3.

Secondary electron image of 12.5 micron repeat grid

A chamber vacuum of < 1x10^-8 mbar is required. If the system does not achieve this, a differentially pumped version should be considered.

Field of view of IOG 25GA is > 2.5 x 2.5 mm

Installation

The IOG 25GA has a compact design, to facilitate its installation on a range of instruments. The envelope of the gun can be varied to meet individual user needs, and the following versions are available:

Standard version (see figure).
Extended nose length, to customer specification.
NW100CF, and other flanged versions.
Differentially pumped version.
Version with bellows for adjusting the length and angle of the gun.

Key dimensions of the IOG 25GA

Optional Equipment

The following items are also available from Ionoptika, for use with the IOG 25GA:

Raster & Imaging Equipment
Fast Beam Pulsing Electronics
Motorised Aperture Drive
Differential Pumping
Mono-isotopic Ga Source
Wien Filter

Principle application	Imaging / Analysis
Energy Range	10 to 25 keV
Min. spot size	50 nm
Max. beam current	20 nA (option for 50 nA)
Max. scan field	1 mm x 1 mm @ 25 kV
Flange to nose length	170 mm
Recommended working distance	25 mm
Rack space required for electronics	6U x 19″ rack mountable unit
Electrical requirements	110-240 VAC 13A 50/60 Hz
Software requirements	PC running Windows 10 or later
Flange type	NW 63 CF

IOG 25AU

February 19, 2018/in News

IOG 25AU

Gold Liquid Metal Ion Beam System

The IOG 25AU is a 25 kV high performance liquid metal ion beam system designed to provide a range of gold and gold-cluster ion beams for SIMS applications. It offers a wide current range with fine probe capability and DC or pulsed operation. Digital control allows easy setup of the gun and a provision for remote control is included.